Online COD analyzers are valuable tools for continuously monitoring water quality in wastewater treatment, industrial effluent control, and environmental protection. To ensure accurate, reliable, and safe operation, paying attention to the following points is crucial.
1. Safety First
Chemical Handling: The analyzer uses strong chemicals (e.g., acids, oxidants like potassium dichromate, which is toxic and carcinogenic). Always wear appropriate Personal Protective Equipment (PPE) like gloves, safety glasses, and a lab coat when handling reagents or maintaining the instrument.
Waste Disposal: Waste generated from the measurement process is hazardous chemical waste. Collect and dispose of it according to your local environmental regulations and safety protocols. Never pour it down the drain.
2. Installation and Sampling
Location: Install the analyzer in a sheltered, well-ventilated area, protected from extreme temperatures and direct sunlight. The environment should be as clean and stable as possible.
Sample Representative: Ensure the sample intake draws a representative sample. The sample line should be free of blockages and leaks. Proper pre-treatment (like filtration) is often necessary to remove large particles or debris that could clog the system. Maintain a consistent sample flow rate and temperature as recommended by the manufacturer.
3. Reagent Management
Quality: Use high-quality reagents of the correct grade specified by the manufacturer. Impure reagents lead to inaccurate results.
Shelf Life: Be aware of the shelf life of reagents. Do not use expired chemicals.
Storage: Store reagents properly according to their requirements (e.g., some may need cool, dark places).
Levels: Regularly check reagent levels and refill or replace them before they run out to prevent pump damage and failed analysis cycles.
4. Calibration and Maintenance
Regular Calibration: Calibrate the instrument regularly as per the manufacturer's schedule using standard COD solutions. This is essential for maintaining accuracy.
Routine Cleaning: Perform routine cleaning of critical components like sample filters, measurement cells, tubing, and electrodes to prevent clogging and fouling. Build-up of dirt or biological growth will cause drift and errors.
Preventative Maintenance: Follow the recommended preventative maintenance schedule. Replace consumable parts (e.g., tubing, seals, valves) before they fail to avoid unexpected downtime.
5. Data Verification
Don't assume the data is always correct. Periodically validate the online analyzer's readings by comparing them with results from standard laboratory COD testing methods on the same sample. Investigate any significant discrepancies immediately.
6. Understanding Limitations
Be aware of the instrument's limitations. Not all online COD analyzers handle very high chloride levels effectively, which can interfere with the measurement. Know the specific operating range and potential interferences for your model.
By following these guidelines—prioritizing safety, ensuring proper sample handling, managing reagents carefully, performing consistent maintenance and calibration, and verifying data—you can maximize the reliability and lifespan of your online COD analyzer, ensuring it provides valuable and accurate data for process control and regulatory compliance.